Serveur d'exploration sur le peuplier

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[Chemical constituents contained in Populus tomentosa].

Identifieur interne : 002847 ( Main/Exploration ); précédent : 002846; suivant : 002848

[Chemical constituents contained in Populus tomentosa].

Auteurs : Haiping Liu [République populaire de Chine] ; Zhimao Chao ; Xiaoyi Wu ; Zhigao Tan ; Chun Wang ; Wen Sun

Source :

RBID : pubmed:22860454

Descripteurs français

English descriptors

Abstract

OBJECTIVE

To separate and identify chemical constituents from stem barks of male plants of Populus tomentosa.

METHOD

Fresh stem barks of P. tomentosa were extracted with methanol to obtain extracts which were suspended in water and blended successively with petroleum ether, ethyl acetate and n-butanol. Various chromatographic techniques were used to separate and purify the constituents extracted with ethyl acetate and n-butanol fractions. Their structures were identified on the basis of their physicochemical properties and spectral data.

RESULT

Twelve compounds were separated with ethyl acetate and n-butanol fractions and identified as benzoic acid (1), daucosterol (2), tremuloidin (3), rhamnocitrin (4), sakuranetin (5), 7-O-methylaromadendrin (6), isograndidentatin A (7), siebolside B (8), sakuranin (9), micranthoside (10), alpha-D-glucopyranose (11), and sucrose (12).

CONCLUSION

Compounds 4-12 were separated from this plant for the first time. Of them, compound 10 was separated from this plant genus for the first time.


PubMed: 22860454


Affiliations:


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Le document en format XML

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<title xml:lang="en">[Chemical constituents contained in Populus tomentosa].</title>
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<name sortKey="Liu, Haiping" sort="Liu, Haiping" uniqKey="Liu H" first="Haiping" last="Liu">Haiping Liu</name>
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<nlm:affiliation>Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences, Beijing 100700, China. liuhaiping0@yahoo.com.cn</nlm:affiliation>
<country xml:lang="fr">République populaire de Chine</country>
<wicri:regionArea>Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences, Beijing 100700</wicri:regionArea>
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<settlement type="city">Pékin</settlement>
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<name sortKey="Chao, Zhimao" sort="Chao, Zhimao" uniqKey="Chao Z" first="Zhimao" last="Chao">Zhimao Chao</name>
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<name sortKey="Wu, Xiaoyi" sort="Wu, Xiaoyi" uniqKey="Wu X" first="Xiaoyi" last="Wu">Xiaoyi Wu</name>
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<name sortKey="Tan, Zhigao" sort="Tan, Zhigao" uniqKey="Tan Z" first="Zhigao" last="Tan">Zhigao Tan</name>
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<name sortKey="Wang, Chun" sort="Wang, Chun" uniqKey="Wang C" first="Chun" last="Wang">Chun Wang</name>
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<name sortKey="Sun, Wen" sort="Sun, Wen" uniqKey="Sun W" first="Wen" last="Sun">Wen Sun</name>
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<term>Flavonoïdes (analyse)</term>
<term>Glucosides (analyse)</term>
<term>Phénols (analyse)</term>
<term>Populus (composition chimique)</term>
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<b>OBJECTIVE</b>
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<p>To separate and identify chemical constituents from stem barks of male plants of Populus tomentosa.</p>
</div>
<div type="abstract" xml:lang="en">
<p>
<b>METHOD</b>
</p>
<p>Fresh stem barks of P. tomentosa were extracted with methanol to obtain extracts which were suspended in water and blended successively with petroleum ether, ethyl acetate and n-butanol. Various chromatographic techniques were used to separate and purify the constituents extracted with ethyl acetate and n-butanol fractions. Their structures were identified on the basis of their physicochemical properties and spectral data.</p>
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<p>
<b>RESULT</b>
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<p>Twelve compounds were separated with ethyl acetate and n-butanol fractions and identified as benzoic acid (1), daucosterol (2), tremuloidin (3), rhamnocitrin (4), sakuranetin (5), 7-O-methylaromadendrin (6), isograndidentatin A (7), siebolside B (8), sakuranin (9), micranthoside (10), alpha-D-glucopyranose (11), and sucrose (12).</p>
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<p>
<b>CONCLUSION</b>
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<p>Compounds 4-12 were separated from this plant for the first time. Of them, compound 10 was separated from this plant genus for the first time.</p>
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